Chinese Journal of Pharmacovigilance ›› 2010, Vol. 7 ›› Issue (8): 449-450.

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Ion Chromatography Determination of Glucosamine Calcium Citrate Dispersible Tablets

HUANG Peng1, ZHANG Xiu-Zhen2, TIAN De-xiang2, FENG Chuan-Ping3   

  1. 1Anhui University of Traditional Chinese Medicine, Anhui Key Laboratory of Modernized Chinese Material, Anhui Hefei 230031, China;
    2College of Chemistry and Chemical Engineering, Anhui University, Anhui Hefei 230001, China;
    3Department of Pharmacy, Hunan College of Traditional Chinese Medicine, Hunan Zhuzhou 412012, China
  • Received:2016-02-22 Revised:2016-02-22 Online:2010-08-08 Published:2016-02-22

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Abstract: Objective To establish an assay method of determination for Glucosamine hydrochloride of Glucosamine Calcium Citrate Dispersible Tablets by ion chromatography(IC). Methods The assay was performed on CarboPacTM PA200 3mm×250mm(with CarboPacTM PA200 3mm×50mm protective column); mobile phase:0.2mol/L NaOH,The flow rate was 0.5mL/min; the column temperaturetemprature 30℃. Results The line ranges of Glucosamine hydro-chloride as partate was 0.01~0.2 mg/L(r=0.9995),The average recoveries of Glucosamine hydrochloride were 99.5%. Conclusion The method is proved to be rapid, accurate, and convenient,and provided a reliable way for evaluating the quality of Glucosamine hydrochloride as Glucosamine Calcium Citrate Dispersible Tablets.

Key words: ion chromatography, glucosamine calcium citrate dispersible tablets, determination

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